People who had direct contact with the water are advised to seek medical advice if they feel unwell.
The affected area of the canal runs from Spinks Bridge to Birchills Street Bridge, Walsall Council saidThe spillage was found on Monday in Pleck, Walsall, according to the local council who said the Environment Agency was first notified of it.
Access to the affected stretch, more than a mile of the canal between Spinks Bridge and Birchills Street Bridge, was closed.
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